Characterization and Synthesis through Fast Phase-Transfer of Oil-Soluble Double-Coordinated Tea-Polyphenols ArsenicReport as inadecuate




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Fast phase-transferring was adopted in ethanol solution at the condition of n oil-soluble tea pol-yphenol: N As3﹢ = 2:1, 4:1, 6:1, pH = 4.0, temperature 40°C - 45°C, action period of 15 h to compose the target, of which the productivity was 59%, UV was 267.50, 218.00, 220.50 nm, FTIR was 6291, 34158.6, 2850.2, 1708.2; 1457.3; 1370.4, 1224.2, 1144.0, 760.5 cm﹣1, fluorescence value λmax = 257, 591.1, 593.7, 590.3, 591.0, 591.5, XRD λ-nm is 3.6974, 4.186, 12.0762, 15.4747, 1H-NMRδ = 0.782, 1.193, 1.483 - 1.586, 1.959 - 2.184, 2.479, 3.116, 3.970 - 3.981, 5.231 - 5.753, 6.537 - 7.300. Finally it was ascertained through XRD as double-coordinated polycrystal compound.

KEYWORDS

Oil-Soluble, Tea-Polyphenols TP, Arsenic Compound, Fast Phase-Transfer, Synthesis, Characterization

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Zhou, W. , Chen, Y. and Zhang, L. 2014 Characterization and Synthesis through Fast Phase-Transfer of Oil-Soluble Double-Coordinated Tea-Polyphenols Arsenic. Journal of Biosciences and Medicines, 2, 34-41. doi: 10.4236-jbm.2014.25004.





Author: Wenfu Zhou, Yahong Chen, Lin Zhang

Source: http://www.scirp.org/



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