Methyl 2-2-{2-2-acetamidophenylethynylbenzamido} phenylethynylbenzoateReport as inadecuate


Methyl 2-2-{2-2-acetamidophenylethynylbenzamido} phenylethynylbenzoate


Methyl 2-2-{2-2-acetamidophenylethynylbenzamido} phenylethynylbenzoate - Download this document for free, or read online. Document in PDF available to download.

1

Division of Organic Chemistry, National Institute of Health Sciences, 1-18-1, Kamiyoga, Setagaya, Tokyo 158-8501, Japan

2

Osaka University of Pharmaceutical Sciences, Osaka 569-1094, Japan





*

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Abstract The title compound was prepared by inducing amide bond formation between methyl 2-2-aminophenylethynylbenzoate and 2-2-acetamidophenylethynylbenzoic acid in the presence of dichlorotriphenylphosphorane. The structure of the synthesized compound was determined on the basis of its 1H-nuclear magnetic resonance NMR, 13C-NMR, and mass spectral data. Furthermore, the compound’s crystal structure is also reported. View Full-Text

Keywords: foldamer; aromatic amide; X-ray crystallographic analysis foldamer; aromatic amide; X-ray crystallographic analysis





Author: Yosuke Demizu 1,* , Takashi Misawa 1, Nanako Yamagata 1, Mitsunobu Doi 2 and Masaaki Kurihara 1,*

Source: http://mdpi.com/



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