3-{5-Bromo-4-pyrrolidin-1-ylpyrimidin-2-yl}aminophenolReport as inadecuate


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Division of Chemistry and Environmental Science, School of Science and the Environment, Faculty of Science and Engineering, Manchester Metropolitan University, John Dalton Building, Chester Street, Manchester M1 5GD, UK

Abstract Re-investigation of the 1H-NMR spectrum reported for 15-bromo-4-oxa-2,9-diaza-12,4-pyrimidine-31,3-benzenacyclononaphane 2 prepared via a Mitsunobu- mediated macroether cyclisation led to a proposed structural isomer 3. The title compound 3 was prepared via a two-step protocol and assigned using 1H, 13C-NMR and LC-MS. View Full-Text

Keywords: macrocyclic ether; Mitsunobu; macrocyclisation macrocyclic ether; Mitsunobu; macrocyclisation

Author: Alan M. Jones

Source: http://mdpi.com/


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