Synthesis and Characterization of the Inclusion Complex of Dicationic Ionic Liquid and β-CyclodextrinReport as inadecuate




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University of Malaya Centre for Ionic Liquids, Department of Chemistry, Faculty of Science, University of Malaya, 50603 Kuala Lumpur, Malaysia





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Abstract The supramolecular structure of the inclusion complex of β-cyclodextrin β-CD with 1,1’,2,2’-tetramethyl-3,3’-p-phenylenedimethylene diimidazolium dibromide TetraPhimBr, a dicationic ionic liquid, has been investigated. The inclusion complex with 1:1 molar ratio was prepared by a kneading method. Fourier transform infrared spectroscopy FTIR, powder X-ray diffraction XRD analysis, 1H NMR and thermogravimetric analysis TGA confirmed the formation of the inclusion complex. The results showed that the host-guest system is a fine crystalline powder. The decomposition temperature of the inclusion complex is lower than that of its parent molecules, TetraPhimBr and β-CD individually. View Full-Text

Keywords: inclusion complex; β-cyclodextrin; dicationic ionic liquid; host-guest system inclusion complex; β-cyclodextrin; dicationic ionic liquid; host-guest system





Author: Puvaneswary Subramaniam * , Sharifah Mohamad and Yatimah Alias

Source: http://mdpi.com/



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