Synthesis, Crystal Structure, and Fungicidal Activity of 5-4-cyclopropyl-5-3-fluorobenzylthio-4H-1,2,4-triazol-3-yl-4-methyl-1,2,3-thiadiazoleReport as inadecuate




Synthesis, Crystal Structure, and Fungicidal Activity of 5-4-cyclopropyl-5-3-fluorobenzylthio-4H-1,2,4-triazol-3-yl-4-methyl-1,2,3-thiadiazole - Download this document for free, or read online. Document in PDF available to download.

Journal of ChemistryVolume 2013 2013, Article ID 306361, 5 pages

Research ArticleCollege of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310014, China

Received 24 October 2012; Accepted 5 December 2012

Academic Editor: Qing Li

Copyright © 2013 Xing-Hai Liu et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

A new 1,2,3-thiadiazole compound was synthesized and characterized. The crystal structure of the title compound C15H14FN5S2, Mr = 347.43 has been determined by single-crystal X-ray diffraction. The crystal is of triclinic, space group P-1 with , ,  Å, α = 89.973°, β = 82.273°, γ = 73.173°, V = 771.33  Å

, Z = 2, F000 = 360, Dc = 1.496 g-cm

, μ = 0.036 mm

, the final R1 = 0.0358, and wR2 = 0.0986 for 2204 observed reflections with . A total of 5697 reflections were collected, of which 2719 were independent . The herbicidal activity of title compound was determined; the results showed that the title compound displayed excellent fungicidal activity.





Author: Xing-Hai Liu, Jian-Quan Weng, and Cheng-Xia Tan

Source: https://www.hindawi.com/



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